Synthesis and crystal structure of N-(3-methyl-5-phenyl-3,5-dihydro-4H-1,2,4-triazol-4-yl)benzamide

ŞAHİN, ONUR; Büyükgüngör, Orhan; Şaşmaz, Selami; Gümrükçüoǧlu, Nurhan; Kantar, Cihan

doi:10.2116/analscix.24.x219

Synthesis and crystal structure of N-(3-methyl-5-phenyl-3,5-dihydro-4H-1,2,4-triazol-4-yl)benzamide

Yazarlar (5)

Prof. Dr. Onur ŞAHİN Ondokuz Mayis Üniversitesi, Türkiye

Orhan Büyükgüngör
Ondokuz Mayis Üniversitesi, Türkiye

Prof. Dr. Selami Şaşmaz Recep Tayyip Erdogan University, Türkiye

Nurhan Gümrükçüoǧlu
Giresun Üniversitesi, Türkiye

Prof. Dr. Cihan Kantar Recep Tayyip Erdogan University, Türkiye

Makale Türü	Diğer (Teknik, not, yorum, vaka takdimi, editöre mektup, özet, kitap krıtiği, araştırma notu, bilirkişi raporu ve benzeri) (SCOPUS dergilerinde yayınlanan teknik not, editöre mektup, tartışma, vaka takdimi ve özet türünden makale)
Dergi Adı	Analytical Sciences X Ray Structure Analysis Online
Dergi ISSN	1348-2238
Makale Dili	İngilizce	Basım Tarihi	01-2008
Kabul Tarihi	–	Yayınlanma Tarihi	01-01-2008
Cilt / Sayı / Sayfa	24 / 9 / –	DOI	10.2116/analscix.24.x219
Makale Linki	https://www.jstage.jst.go.jp/article/analscix/24/0/24_0_x219/_pdf
UAK Araştırma Alanları	Yoğun Madde Fiziği

Özet

The title compound, N-(3-methyl-5-phenyl-3,5-dihydro-4H-1,2,4-triazol-4-yl)benzamide, C16H14N4O, crystallizes in the monoclinic space group P21/c with the following unit cell parameters: a = 10.6011(6)Å, b = 7.5676(4)Å, c = 19.6363(11)Å, β = 95.062(5)° and Z = 4. Molecules are linked principally by O-H···N hydrogen bonds involving the water OH2 group and a triazole N atom, forming R4⁴(10) and R4⁴(14) rings, which link to give a one-dimensional network of molecules. An extensive two-dimensional network of N-H···O, C-H···O and O-H···N hydrogen bonds, with π-π and π- ring interactions, are responsible for crystal stabilization. 2008 © The Japan Society for Analytical Chemistry.

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Synthesis and crystal structure of N-(3-methyl-5-phenyl-3,5-dihydro-4H-1,2,4-triazol-4-yl)benzamide

Synthesis and crystal structure of N-(3-methyl-5-phenyl-3,5-dihydro-4H-1,2,4-triazol-4-yl)benzamide

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