Synthesis, Spectroscopic Characterization, Single-Crystal Structure, Hirshfeld Surface Analysis, and Antimicrobial Studies of 3-Acetoxy-2-methylbenzoic Anhydride
Yazarlar (6)
Doç. Dr. Şükriye ÇAKMAK Sinop Üniversitesi, Türkiye
Dr. Öğr. Üyesi Sevgi Kansız Samsun University, Türkiye
Mohammad Azam
College Of Sciences, Suudi Arabistan
College Of Sciences, Suudi Arabistan
Doç. Dr. Aysel VEYİSOĞLU Sinop Üniversitesi, Türkiye
Doç. Dr. Hasan Yakan Ondokuz Mayis Üniversitesi, Türkiye
Kim Min
Dongguk University, Gyeongju, Güney Kore
Dongguk University, Gyeongju, Güney Kore
| Makale Türü |
Özgün Makale
(SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale)
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| Dergi Adı | ACS Omega (Q2) | ||
| Dergi ISSN | 2470-1343 Dergi Bilgileri (2022) | ||
| Dergi Tarandığı Indeksler | SCI-Expanded | ||
| Makale Dili | İngilizce | Basım Tarihi | 05-2022 |
| Cilt / Sayı / Sayfa | 7 / 20 / 17192–17201 | DOI | 10.1021/ACSOMEGA.2C00879 |
| Makale Linki | http://dx.doi.org/10.1021/acsomega.2c00879 | ||
| UAK Araştırma Alanları |
Organik Kimya
Spektroskopi
Teorik Kimya
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| Özet |
| We report a novel anhydride derivative, 3-acetoxy-2-methylbenzoic anhydride (AMA), obtained from the interaction of 3-acetoxy-2-methylbenzoyl chloride with 3-acetoxy-2-methylbenzoic acid. The synthesized compound was characterized by elemental analysis, IR, 1H NMR, and 13C NMR spectroscopic studies and single-crystal X-ray crystallography which revealed the crystallization of AMA as monoclinic with space group P21/c. A Hirshfeld surface analysis was performed to record various intermolecular interactions, indicating the stabilization of the AMA structure by the intermolecular weak C–H···O hydrogen bonds and π···π interactions. The title compound was screened for antibacterial and antifungal activities using a serial dilution technique under aseptic conditions. The results indicate that the title compound has significant antibacterial properties but showed no antifungal behavior. |
| Anahtar Kelimeler |
BM Sürdürülebilir Kalkınma Amaçları
| Atıf Sayıları | |
| Web of Science | 14 |
| Scopus | 12 |
| Google Scholar | 12 |