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| Dergi Adı | Cumhuriyet Science Journal | ||
| Dergi ISSN | 2587-2680 | ||
| Dergi Tarandığı Indeksler | TR DİZİN | ||
| Makale Dili | İngilizce | Basım Tarihi | 01-2021 |
| Cilt / Sayı / Sayfa | 42 / 1 / 22–29 | DOI | 10.17776/csj.812164 |
| Makale Linki | http://dx.doi.org/10.17776/csj.812164 | ||
| UAK Araştırma Alanları |
Yoğun Madde Fiziği
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| Özet |
| Herein a novel inorganic-organic hybrid Keggin-type heteropolymolybdate [Ni2Na (C12H8N2) 4 (BMo12O40)(H2O) 2](1) has been synthesized under hydrothermal conditions in aqueous solution. The cyrstal structure was fully characterized by powder X-ray diffraction (XRD), elemental analysis, Fourier-tranform infrared spectrum (FT-IR), Thermogravimetric analysis (TGA) and Scanning Electron Microscopy (SEM) analysis. Single crystal X-ray structural analysis demonstrates that the complex consists of a Keggin anion [BMo12O40] 5− polyanion, four 1, 10-phenanthroline (C12H8N2) ligands, two Ni (II) ions, two Na (I) ions and two aqua ligands. The experimental powder X-ray diffraction (XRD) result of the crystal is consistent with the calculated data. The SEM image shows that the compound crystals have a cubic structure. |
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| Google Scholar | 4 |